Sintesis Anisol Menggunakan N-Setil N,N,N-Trim Etil Ammonium Bromida sebagai Katalis Transfer Fasa

Enny Fachriyah; Damin Sumardjo; Sausan Syakib Arsalan

doi:10.14710/jksa.2.4.118-121

DOI: https://doi.org/10.14710/jksa.2.4.118-121

Sintesis Anisol Menggunakan N-Setil N,N,N-Trim Etil Ammonium Bromida sebagai Katalis Transfer Fasa

Enny Fachriyah

, Damin Sumardjo, Sausan Syakib Arsalan

Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University, Indonesia

Published: 30 Nov 1999.

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Abstract

Telah dilakukan sintesis anisol dengan cara mereaksikan fenol, natrium hidroksida dan dimetil sulfat dalam pelarut metilen klorida dengan N-setil-N,N,N-trimetil amonium bromida digunakan sebagai katalis transfer fasa. Hasil sintesis yang diperoleh ditentukan indeks bias dan bobot jenisnya serta dilakukan analisis dengan kromatografi gas dan spektroskopi infra merah. Hasil yang diperoleh mempunyai indeks bias pada 20°C (n_D²⁰) sebesar 1,51025 dan bobot jenis pada 18°C (ρ¹⁸) sebesar 0,99725. Analisa dengan kromatografi gas menunjukkan kemurnian 98,68% dengan spektroskopi infra merah menunjukkan adanya gugus – OCH₃ dan gugus aromatik. Diperkirakan produk adalah anisol.

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Keywords: Anisol; katalis transfer fasa; N-cetyl-N,N,N-trimethylammonium bromide

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Section: Research Articles

Language : ID

In Vol 2, No 4 (1999): Volume 2 Issue 4 Year 1999

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Retno Dwi Soelisyowati, 1985, “Optimasi Sintesis Metil Eugenol dari Cengkeh Memakai Katalis Transfer Fasa dalam Media Pelarut Organik” Laboratorium Kimia Organik F.MIPA Universitas Gadjah Mada Yogyakarta , Halaman 9- 11
Gokel, George, W. and Weber, William P., Phase Transfer Catalysis. J. Chem. Education, 55(6), 350(1978)
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Silverstein, R.M., Bassler, Clayton, G. and Morrill, Terence, C., 1991, Spectrometric Identification of Organic Compounds, Fifth Edition, John Wiley and Sons., Inc., New York, Page 113

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