Enhancing the Quality of Patchouli Oil using Zeolite and Bentonite Nano-Particle Adsorbents

Suraiya Kamaruzzaman; Syaifullah Muhammad; Sri Aprilia; Rahmat Alfano; Muhammad Ridha; Yanna Syamsuddin; Hesti Meilina

doi:10.14710/jksa.24.7.259-267

DOI: https://doi.org/10.14710/jksa.24.7.259-267

Enhancing the Quality of Patchouli Oil using Zeolite and Bentonite Nano-Particle Adsorbents

Suraiya Kamaruzzaman

, Syaifullah Muhammad

, Sri Aprilia

, Rahmat Alfano, Muhammad Ridha, Yanna Syamsuddin

, Hesti Meilina

Department of Chemical Engineering, Universitas Syiah Kuala, Banda Aceh, Indonesia

Received: 24 May 2021; Revised: 5 Jul 2021; Accepted: 20 Nov 2021; Published: 31 Dec 2021.

BibTex Citation Data :

@article{JKSA38544,
    author = {Suraiya Kamaruzzaman and Syaifullah Muhammad and Sri Aprilia and Rahmat Alfano and Muhammad Ridha and Yanna Syamsuddin and Hesti Meilina},
    title = {Enhancing the Quality of Patchouli Oil using Zeolite and Bentonite Nano-Particle Adsorbents},
    journal = {Jurnal Kimia Sains dan Aplikasi},
  volume = {24},
    number = {7},
    year = {2021},
    keywords = {Adsorption; nano zeolite; nano bentonite; Fe2+ metal ions, patchouli oil},
    abstract = { The overall quality of patchouli oil is closely related to the purification process during manufacturing. This research provided an effective and efficient method for purifying Aceh patchouli oil to secure high-quality patchouli oil. Purification was done by utilizing natural mineral sources that were sufficiently available in Aceh and applying them in various adsorption processes, analyzing the adsorption of Fe levels in patchouli oil, and characterizing nano adsorbents used in the adsorption process. Nanoparticles of zeolite and bentonite were used during the adsorption process with patchouli oil sourced from the South Aceh area. The adsorption process purified 20 mL of patchouli oil at a temperature of 45 ℃ with variable mass nano adsorbent 1; 3; 5 g, and variable stirring time 60; 180; 300 minutes. The purification filtrate was later analyzed for patchouli alcohol levels using Gas Chromatography-Mass Spectrometry (GC-MS) and Fe levels using UV-Vis Spectrophotometry. The characterization of nano adsorbents was conducted using Scanning Electron Microscopy (SEM) and X-ray Diffractometry (XRD). The results showed that the most efficient adsorption process occurred in nano zeolite with a mass of 5 g and a stirring time of 300 minutes, where the patchouli alcohol content was 28.54%, Fe 0.8165 mg/kg. Meanwhile, nano zeolite’s most significant constituent components were silicon oxide (SiO 2 ) of 48.9% and silicon carbide (CSi) of 31.3%. Visually the sample did not change color due to the low quality of patchouli oil, but the Fe level in the patchouli oil samples complied with SNI 06-2385-2006 with a maximum of 25 mg/kg. In addition, nano zeolite had an adsorption capacity of 0.96 mg/g with an adsorption efficiency of 98.49%. },
   issn = {2597-9914},   pages = {259--267}  doi = {10.14710/jksa.24.7.259-267},
    url = {https://ejournal.undip.ac.id/index.php/ksa/article/view/38544}
}

Citation Format:

Abstract

The overall quality of patchouli oil is closely related to the purification process during manufacturing. This research provided an effective and efficient method for purifying Aceh patchouli oil to secure high-quality patchouli oil. Purification was done by utilizing natural mineral sources that were sufficiently available in Aceh and applying them in various adsorption processes, analyzing the adsorption of Fe levels in patchouli oil, and characterizing nano adsorbents used in the adsorption process. Nanoparticles of zeolite and bentonite were used during the adsorption process with patchouli oil sourced from the South Aceh area. The adsorption process purified 20 mL of patchouli oil at a temperature of 45 ℃ with variable mass nano adsorbent 1; 3; 5 g, and variable stirring time 60; 180; 300 minutes. The purification filtrate was later analyzed for patchouli alcohol levels using Gas Chromatography-Mass Spectrometry (GC-MS) and Fe levels using UV-Vis Spectrophotometry. The characterization of nano adsorbents was conducted using Scanning Electron Microscopy (SEM) and X-ray Diffractometry (XRD). The results showed that the most efficient adsorption process occurred in nano zeolite with a mass of 5 g and a stirring time of 300 minutes, where the patchouli alcohol content was 28.54%, Fe 0.8165 mg/kg. Meanwhile, nano zeolite’s most significant constituent components were silicon oxide (SiO₂) of 48.9% and silicon carbide (CSi) of 31.3%. Visually the sample did not change color due to the low quality of patchouli oil, but the Fe level in the patchouli oil samples complied with SNI 06-2385-2006 with a maximum of 25 mg/kg. In addition, nano zeolite had an adsorption capacity of 0.96 mg/g with an adsorption efficiency of 98.49%.

Fulltext View|Download Email colleagues

Keywords: Adsorption; nano zeolite; nano bentonite; Fe2+ metal ions, patchouli oil

Funding: Universitas Syiah Kuala

Article Metrics:

Article Info

Section: Research Articles

Language : EN

In Vol 24, No 7 (2021): Volume 24 Issue 7 Year 2021

Most cited articles

Dealuminasi Zeolit Alam Cipatujah Melalui Penambahan Asam dan Oksidator Molecular Docking of Interaction between E-Cadherin Protein and Conformational Structure of Cyclic Peptide ADTC3 (Ac-CADTPC-NH2) Simulated on 20 ns Antioxidant Activity of Daemonorops draco Resin Asam Anakardat dari Kulit Biji Jambu Mete (Anacardium Occidentale L) yang Mempunyai Aktivitas Sitotoksik Synthesis of Alginate-Chitosan Polyelectrolyte Complex (PEC) Membrane and Its Physical-Mechanical Properties More cited articles

Niken Harimurti, Tatang H Soerawidjaja, Djajeng Sumangat, Ekstraksi Minyak Nilam (Pogostemon cablin Benth) dengan Teknik Hidrodifusi Pada Tekanan 1–3 Bar, Jurnal Penelitian Pascapanen Pertanian, 9, 1, (2013), 1-10
Bappeda, Action Plan Sistem Inovasi Industri Nilam Aceh, (2015)
Tri Widayatno, Teti Yuliawati, Agung A Susilo, Adsorpsi logam berat (Pb) dari limbah cair dengan adsorben arang bambu aktif, Jurnal teknologi bahan alam, 1, 1, (2017), 17-23
Lisanti Emelda, Suhardini Martiana Putri, Simparmin Ginting, Pemanfaatan zeolit alam teraktivasi untuk adsorpsi logam Krom (Cr3+), Jurnal Rekayasa Kimia & Lingkungan, 9, 4, (2013), 166-172 https://doi.org/10.23955/rkl.v9i4.1229
Ratri Ariatmi Nugrahani, Ismiyati Ismiyati, Pemanfaatan Nanobentonit sebagai Bahan Tambahan pada Formula Grease, Kosmetik dan Nanokomposit Polimer, Seminar Nasional Sains dan Teknologi, Jakarta, 2014
Daniel S Bath, Jenal M Siregar, M Turmuzi Lubis, Penggunaan tanah bentonit sebagai adsorben logam Cu, Jurnal Teknik Kimia USU, 1, 1, (2012), 1-4 https://doi.org/10.32734/jtk.v1i1.1396
Badan Standarisasi Nasional, Standar Nasional Indonesia, Minyak Nilam, SNI 06-2385-2006, Jakarta, 2006
Dessy Kurniasari, Sri Atun, Pembuatan dan karakterisasi nanopartikel ekstrak etanol temu kunci (boesenbergia pandurata) pada berbagai variasi komposisi kitosan, Jurnal Sains Dasar, 6, 1, (2017), 31-35 https://doi.org/10.21831/jsd.v6i1.13610
Sariadi, Permunian Minyak Nilam dengan Proses Adsorpsi Menggunakan Bentonit, Jurnal Teknologi, 12, 2, (2012), 100-104
Mega Roikhanah Fauziyati, Uji Adsorpsi Bentonit Teraktivasi KOH Terhadap Logam Cu (II), Walisongo Journal of Chemistry, 2, 2, (2019), 80-88 https://doi.org/10.21580/wjc.v2i2.6028
Ummul Habibah Hasyim, Pengaruh Konsentrasi HCl dan Massa Adsorbent dalam Pengolahan Limbah Pelumas Bekas dengan Kajian Keseimbangan Adsorpsi Bentonit terhadap Logam Fe, Jurnal Integrasi Proses, 6, 4, (2017), 191-196 http://dx.doi.org/10.36055/jip.v6i4.2545
Ika Sri Hardyanti, H. Hp Dyan Septyaningsih, Nurani Isni, Wibowo Emas Agus Prastyo, Analisis Kadar Patchouli Alcohol menggunakan Gas Chromatography pada Pemurnian Minyak Nilam menggunakan Adsorben Zeolit, Prosiding Seminar Nasional XI Rekayasa Teknologi Industri dan Informasi, Yogyakarta, 2016

Last update:

Performances of patchouli oil purification through adsorption process
Suraiya, Syaifullah Muhammad, Aula Chairunnisak, Darmadi, Syawaliah Muchtar. THE 12TH ANNUAL INTERNATIONAL CONFERENCE (AIC) 2022: The 12th Annual International Conference on Sciences and Engineering (AIC-SE) 2022, 3082 , 2024. doi: 10.1063/5.0201620

Last update: 2026-09-19 05:08:11

No citation recorded.

As an article writer, the author has the right to use their article for various purposes, including use by institutions that employ the author or institutions that provide funding for the research. These author rights are granted without special permission.

Authors who publish a paper in JKSA have broad rights to use their work for teaching and scientific purposes without the need to request permission, including: (i) teaching in the author's class or institution; (ii) presenting the work at meetings or conferences and distributing copies to participants; (iii) using the work in training conducted by the author or the author's institution; (iv) distributing copies to colleagues for research purposes; (v) using the work in the compilation of subsequent works by the author; (vi) including the work in a thesis or dissertation; (vii) reusing part of the article in another work, with appropriate citation; (viii) preparing derivative works, with appropriate citation; and (ix) voluntarily posting the work on open websites operated by the author or the author's institution for scientific purposes, in accordance with the CC BY-SA License.

Authors and readers may copy and redistribute the material in any medium or format, and may remix, transform, and build upon the material for any purpose, provided that they give appropriate credit by citing the article or its content, provide a link to the license, and indicate if changes were made.

The authors submitting a manuscript do so on the understanding that, if accepted for publication, the copyright of the article shall be assigned to Jurnal Kimia Sains dan Aplikasi (JKSA). Copyright encompasses the rights to reproduce and distribute the article in all forms and media, including reprints, photographs, microfilms, and any other similar reproductions, as well as translations.

Reproducing any part of this journal, storing it in a database, or transmitting it in any form or medium is permitted without written permission from JKSA. However, the original source must be properly cited in accordance with academic conventions.

JKSA, the Chemistry Department of Diponegoro University, and the Editor make every effort to ensure that no inaccurate, false, or misleading data, opinions, or statements are published in JKSA. However, the content of each article is the sole and exclusive responsibility of its authors.

The Copyright Transfer Form can be downloaded here: [Copyright Transfer Form - Indonesian] [Copyright Transfer Form - English]. The copyright form should bear the authors' original signatures and be sent to the Editor as a printed document, a scanned document sent via email, or by fax.

Prof. Adi Darmawan, Ph.D (Editor in Chief)

Editor in chief of Jurnal Kimia Sains dan Aplikasi (JKSA)

Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Jl. Prof. Soedarto, Kampus Undip Tembalang, Semarang, Central Java, Indonesia 50275
Email: jksa@live.undip.ac.id