skip to main content

Study on the Upgrading Citronella (Cymbopogon nardus L.) Oil Isolation Using Microwave Assisted Hydro-distillation Method

1Department of Chemical Engineering, Faculty of Industrial Engineering, Universitas Islam Indonesia, Yogyakarta, Indonesia

2Department of Chemical Engineering, Faculty of Industrial Technology, Institut Teknologi Bandung, Bandung, Indonesia

Received: 27 Oct 2023; Revised: 5 Apr 2024; Accepted: 18 Apr 2024; Published: 30 Jun 2024.
Open Access Copyright 2024 Jurnal Kimia Sains dan Aplikasi under http://creativecommons.org/licenses/by-sa/4.0.

Citation Format:
Cover Image
Abstract
Isolation of essential oil using microwave-assisted hydro-distillation (MAHD) method could enhance the yield compared to steam-distillation or conventional hydro-distillation methods. This study explored the isolation of essential oil from Citronella (Cymbopogon nardus L.) using the MAHD method with several parameters, such as solid-to-liquid ratio, power of the microwave, and extraction time. The essential oils produced were evaluated based on yield, density, refractive index, and composition. The result showed that the density of the essential oil product was in the range of 0.866–0.902 g/mL, while the refractive index was in the range of 1.470–1.475, which met the ISO standard. Chemical compounds were identified using Gas Chromatography-Mass Spectrometry (GC-MS) analysis. It was found that the total amount of citronellal, citronellol, and geraniol in the product obtained by MAHD is higher than the one from conventional methods. This study aims to identify the most efficient operating conditions to maximize yield while analyzing energy consumption to determine the most cost-effective conditions.
Fulltext View|Download
Keywords: Upgrading; isolation; citronella oil; microwave-assisted hydro-distillation
Funding: The Indonesian Ministry of Education, Culture, Research and Technology; Department of Chemical Engineering, Universitas Islam Indonesia

Article Metrics:

  1. H. Sastrohamidjojo, Kimia Minyak Atsiri, Gadjah Mada University Press, Yogyakarta, 2014,
  2. Anny Sulaswatty, Quo vadis minyak serai wangi dan produk turunannya, LIPI Press, Jakarta, 2019,
  3. Sri Mulyani, Purwanto, Sudarsono, Wahyono, Suwijiyo Pramono, Indah Purwantini, Andayana Puspitasari G., Djoko Santosa, Triana Hertiani, Nanang Fakhrudin, Yosi Bayu Murti, Sylvia Utami, Minyak Atsiri Tumbuhan Obat, Gadjah Mada University Press, Yogyakarta, 2020,
  4. Babar Ali, Naser Ali Al-Wabel, Saiba Shams, Aftab Ahamad, Shah Alam Khan, Firoz Anwar, Essential oils used in aromatherapy: A systemic review, Asian Pacific Journal of Tropical Biomedicine, 5, 8, (2015), 601-611 https://doi.org/10.1016/j.apjtb.2015.05.007
  5. Vikrant P. Katekar, Anand B. Rao, Vishal R. Sardeshpande, A hydrodistillation-based essential oils extraction: A quest for the most effective and cleaner technology, Sustainable Chemistry Pharmacy, 36, (2023), 101270 https://doi.org/10.1016/j.scp.2023.101270
  6. Ravi Kant, Anil Kumar, Review on essential oil extraction from aromatic and medicinal plants: Techniques, performance and economic analysis, Sustainable Chemistry and Pharmacy, 30, (2022), 100829 https://doi.org/10.1016/j.scp.2022.100829
  7. E. T. Thostenson, T. W. Chou, Microwave processing: fundamentals and applications, Composites Part A: Applied Science and Manufacturing, 30, 9, (1999), 1055-1071 https://doi.org/10.1016/S1359-835X(99)00020-2
  8. Sibel Karakaya, Sedef Nehir El, Nural Karagozlu, Serpil Sahin, Gulum Sumnu, Beste Bayramoglu, Microwave-assisted hydrodistillation of essential oil from rosemary, Journal of Food Science and Technology, 51, 6, (2014), 1056-1065 https://doi.org/10.1007/s13197-011-0610-y
  9. Fengli Chen, Yuangang Zu, Lei Yang, A novel approach for isolation of essential oil from fresh leaves of Magnolia sieboldii using microwave-assisted simultaneous distillation and extraction, Separation and Purification Technology, 154, (2015), 271-280 https://doi.org/10.1016/j.seppur.2015.09.066
  10. Mohd Nazarni Che Isa, Azilah Ajit, Aishath Naila, A. Z. Sulaiman, Effect of microwave assisted hydrodistillation extraction on extracts of Ficus deltoidea, Materials Today: Proceedings, 5, 10, Part 2, (2018), 21772-21779 https://doi.org/10.1016/j.matpr.2018.07.031
  11. Siti Sarah Mohamad Zaid, Shatrah Othman, Normadiah M. Kassim, Protective role of Mas Cotek (Ficus deltoidea) against the toxic effects of bisphenol A on morphology and sex steroid receptor expression in the rat uterus, Biomedicine & Pharmacotherapy, 140, (2021), 111757 https://doi.org/10.1016/j.biopha.2021.111757
  12. Megawati, Dewi Selvia Fardhyanti, Wahyudi Budi Sediawan, Anwaruddin Hisyam, Kinetics of mace (Myristicae arillus) essential oil extraction using microwave assisted hydrodistillation: Effect of microwave power, Industrial Crops and Products, 131, (2019), 315-322 https://doi.org/10.1016/j.indcrop.2019.01.067
  13. Thien Hien Tran, Duy Chinh Nguyen, Thuong Nhan Nguyen Phu, Van Thi Thanh Ho, Dai Viet Nguyen Vo, Long Giang Bach, Trinh Duy Nguyen, Research on Lemongrass Oil Extraction Technology (Hydrodistillation, Microwave-Assisted Hydrodistillation), Indonesian Journal of Chemistry, 19, 4, (2019), 1000-1007 https://doi.org/10.22146/ijc.40883
  14. Mohamed Nadjib Boukhatem, Mohamed Amine Ferhat, Mehdi Rajabi, Shaker A. Mousa, Solvent-free microwave extraction: an eco-friendly and rapid process for green isolation of essential oil from lemongrass, Natural Product Research, 36, 2, (2022), 664-667 https://doi.org/10.1080/14786419.2020.1795852
  15. Piyush I. Modi, Jigisha K. Parikh, Meghal A. Desai, Intensified approach towards isolation of cinnamon oil using microwave radiation: Parametric, optimization and comparative studies, Industrial Crops and Products, 173, (2021), 114088 https://doi.org/10.1016/j.indcrop.2021.114088
  16. Heri Septya Kusuma, Mahfud Mahfud, The extraction of essential oils from patchouli leaves (Pogostemon cablin Benth) using a microwave air-hydrodistillation method as a new green technique, RSC Advances, 7, 3, (2017), 1336-1347 https://doi.org/10.1039/C6RA25894H
  17. Heri Septya Kusuma, Mahfud Mahfud, Microwave-assisted hydrodistillation for extraction of essential oil from patchouli (Pogostemon cablin) leaves, Periodica Polytechnica Chemical Engineering, 61, 2, (2017), 82-92 https://doi.org/10.3311/PPch.8676
  18. Sirinat Noyraksa, Kittisak Wichianwat, Sirinya Punpuk, Supakorn Aiemyeesun, Jakkrawut Maitip, Panawan Suttiarporn, Optimization of microwave-assisted hydrodistillation of essential oils from fennel seeds, Materials Today: Proceedings, 77, (2023), 1079-1085 https://doi.org/10.1016/j.matpr.2022.11.392
  19. Hayet Boudraa, Nabil Kadri, Lotfi Mouni, Khodir Madani, Microwave-assisted hydrodistillation of essential oil from fennel seeds: Optimization using Plackett–Burman design and response surface methodology, Journal of Applied Research on Medicinal and Aromatic Plants, 23, (2021), 100307 https://doi.org/10.1016/j.jarmap.2021.100307
  20. Edwin Fatah Daniswara, Taufik Imam Rohadi, Mahfud Mahfud, Ekstraksi Minyak Akar Wangi dengan Metode Microwave Hydrodistillation dan Soxhlet Extraction, Jurnal Teknik ITS, 6, 2, (2017), F381-F384 http://dx.doi.org/10.12962/j23373539.v6i2.24483

Last update:

No citation recorded.

Last update: 2024-07-17 18:33:31

No citation recorded.