Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University, Indonesia
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@article{JKSA3319, author = {Ngadiwiyana Ngadiwiyana and Ismiyarto Ismiyarto and Ahmad Fathoni}, title = {Sintesis 3-(3,4-Dimetoksi Fenil)-1-Propanol Melalui Hidroborasi Metileugenol Menggunakan H3B:Dietileter}, journal = {Jurnal Kimia Sains dan Aplikasi}, volume = {8}, number = {1}, year = {2005}, keywords = {Metileugenol; Hidroborasi; Borana}, abstract = {Penelitian ini merupakan usaha untuk meningkatkan nilai guna dari minyak daun cengkeh dengan memanfaatkan kandungan utamanya yaitu eugenol. Eugenol dapat diubah menjadi metileugenol lalu dikonversi menjadi 3-(3,4-dimetoksi fenil)-1-propanol melalui reaksi hidroborasi dengan menggunakan reagen H 3 B:dietileter. Kemudian, dioksidasi menggunakan hidrogen peroksida yang diikuti dengan hidrolisis dalam suasana basa untuk memperoleh alkohol. Produk sintesis dianalisis menggunakan spektrometer FTIR dan GC-MS. Data spektra FTIR memperlihatkan serapan kuat oleh gugus hidroksil pada bilangan gelombang 3448,5 cm -1 . Hal ini menunjukkan bahwa senyawa 3-(3,4-dimetoksifenil)-1-propanol telah terbentuk. Hasil ini diperkuat oleh pola fragmentasi senyawa pada data MS yang menunjukkan adanya puncak dasar dengan m/z = 151 dan ion molekul dengan m/z = 196 yang merupakan berat molekul dari senyawa 3-(3,4-dimetoksi fenil)-1-propanol. Produk sintesis yang diperoleh memiliki rendemen mencapai 81,29%. Selanjutnya, senyawa ini digunakan sebagai senyawa antara dalam sintesis turunan antibiotik C-9154}, issn = {2597-9914}, pages = {9--16} doi = {10.14710/jksa.8.1.9-16}, url = {https://ejournal.undip.ac.id/index.php/ksa/article/view/3319} }
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