Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University, Indonesia
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@article{JKSA17923, author = {Medina Indriati and Rahmad Nuryanto and Linda Suyati}, title = {Pengaruh Suhu Kalsinasi terhadap Konduktivitas dan Kristalinitas Elektrolit Padat NaMn2-xMgxO4}, journal = {Jurnal Kimia Sains dan Aplikasi}, volume = {16}, number = {2}, year = {2013}, keywords = {Elektrolit padat; metode sol-gel; kalsinasi; konduktivitas; kristalinitas}, abstract = {Telah dilakukan pembuatan elektrolit padat NaMn 2-x Mg x O 4 melalui metode sol-gel dengan variasi suhu kalsinasi. Penelitian ini bertujuan untuk menentukan suhu kalsinasi optimum dalam pembuatan elektrolit padat NaMn 2-x Mg x O 4 dan karakterisasi elektrolit padat NaMn 2-x Mg x O 4 menggunakan FTIR dan XRD. Elektrolit padat NaMn 2-x Mg x O 4 dibuat dengan mencampurkan larutan natrium asetat, mangan asetat, magnesium asetat, dan asam sitrat, kemudian dilakukan pengadukan, penguapan pada suhu 80°C, pengeringan gel pada suhu 180°C, dan kalsinasi pada berbagai variasi suhu, yaitu 700, 750, 800, 850, dan 900°C. Uji konduktivitas elektrolit padat dilakukan melalui pengukuran tahanan menggunakan multimeter, kemudian elektrolit padat dengan nilai konduktivitas tertinggi dan terendah dikarakterisasi menggunakan FTIR untuk menentukan interaksi antar atom-atom dalam elektrolit padat NaMn 2-x Mg x O 4 dan XRD untuk menentukan kristalinitas elektrolit padat NaMn 2-x Mg x O 4 . Data konduktivitas menunjukkan bahwa suhu 800°C merupakan suhu kalsinasi yang optimum, sedangkan data FTIR dan XRD menunjukkan bahwa elektrolit padat yang terbentuk adalah padatan kristal NaMn 2-x Mg x O 4 dan kristalinitas sampel 900°C lebih tinggi dari sampel 800°C.}, issn = {2597-9914}, pages = {46--49} doi = {10.14710/jksa.16.2.46-49}, url = {https://ejournal.undip.ac.id/index.php/ksa/article/view/17923} }
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