Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University, Indonesia
BibTex Citation Data :
@article{JKSA21611, author = {Abdul Haris and Gunawan Gunawan and Didik Widodo and Rahmad Nuryanto and Retno Lusiana and Mei Viantikasari}, title = {Synthesis, Characterization of Cu, S doped TiO2 and Its Photocatalytic Activity for Degradation of Remazol Black B}, journal = {Jurnal Kimia Sains dan Aplikasi}, volume = {22}, number = {2}, year = {2019}, keywords = {Cu, S doped TiO2; photocatalytic; degradation; remazol black B}, abstract = { Copper and sulfur modified TiO 2 (Cu-S-TiO 2 ) photocatalyst was successfully synthesized using TiCl 4 , Cu(NO 3 ) 2 .3H 2 O and H 2 SO 4 as precursors by the sol-gel method andcalcination at 450 ° C for 4 hours. The synthesized photocatalyst was characterized by X-Ray Diffraction (XRD), Scanning Electron Microscopy-Energy Dispersive Spectroscopy (SEM-EDS), Diffuse Reflectance Spectroscopy (DRS), Brunauer Emmett Teller (BET) method. The XRD results showed that the Cu-S-TiO 2 photocatalyst had an anatase phase with a crystal grain size of 17.54 nm. However, the SEM image of the modified TiO 2 showed in homogeneous phase due to the crystal clustering of imperfect homogenization during the synthesis and sintering processes . The patterns of EDSof Cu-S-TiO 2 depicted the elements of Ti, O, Cu and S with doping of Cu and S c.a. 7 and 1%, respectively. Analysis using DRS UV-Vis showed Cu-S-TiO 2 was able to shift the absorption of the TiO 2 photocatalyst wavelength to the visible region with a band energy gap of 1.9 eV. The BET analysis results showed that the specific surface area (S BET ), pore volume (V p ) and average pore volume radius (D p ) were measured from large Cu-S-TiO 2 , therefore Cu-S-TiO 2 had good physicochemical and photocatalytic properties. The photocatalytic activity of 0.1 g Cu-S-TiO 2 with 15 Watt tungsten light irradiation for 4 h was able to degrade 50 mL remazol black B 10 mg/L c.a. 92.60 %. }, issn = {2597-9914}, pages = {47--51} doi = {10.14710/jksa.22.2.47-51}, url = {https://ejournal.undip.ac.id/index.php/ksa/article/view/21611} }
Refworks Citation Data :
Copper and sulfur modified TiO2(Cu-S-TiO2) photocatalyst was successfully synthesized using TiCl4, Cu(NO3)2.3H2O and H2SO4 as precursors by the sol-gel method andcalcination at 450°C for 4 hours. The synthesized photocatalyst was characterized by X-Ray Diffraction (XRD), Scanning Electron Microscopy-Energy Dispersive Spectroscopy (SEM-EDS), Diffuse Reflectance Spectroscopy (DRS), Brunauer Emmett Teller (BET) method. The XRD results showed that the Cu-S-TiO2 photocatalyst had an anatase phase with a crystal grain size of 17.54 nm. However, the SEM image of the modified TiO2 showed inhomogeneous phase due to the crystal clustering of imperfect homogenization during the synthesis and sintering processes. The patterns of EDSof Cu-S-TiO2depicted the elements of Ti, O, Cu and S with doping of Cu and S c.a. 7 and 1%, respectively. Analysis using DRS UV-Vis showed Cu-S-TiO2 was able to shift the absorption of the TiO2 photocatalyst wavelength to the visible region with a band energy gap of 1.9 eV. The BET analysis results showed that the specific surface area (SBET), pore volume (Vp) and average pore volume radius (Dp) were measured from large Cu-S-TiO2, therefore Cu-S-TiO2 had good physicochemical and photocatalytic properties. The photocatalytic activity of 0.1 g Cu-S-TiO2 with 15 Watt tungsten light irradiation for 4 h was able to degrade 50 mL remazol black B 10 mg/L c.a. 92.60 %.
Article Metrics:
Last update:
Efficient photocatalysis of carbon coupled TiO2 to degrade pollutants in wastewater – A review
The Effect of Cu Ohmic Contact on Photoelectrochemical Property of S-CuO Thin Film Photocathodes
Last update: 2024-04-18 05:20:19
As an article writer, the author has the right to use their articles for various purposes, including use by institutions that employ authors or institutions that provide funding for research. Author rights are granted without special permission.
Author who publishes a paper at JKSA has the broad right to use their work for teaching and scientific purposes without the need to ask permission, including: used for (i) teaching in the author's class or institution, (ii) presentation at meetings or conferences and distributing copies to participants ; (iii) training conducted by the author or author's institution; (iv) distribution to colleagues for research use; (v) use in the compilation of subsequent authors' works; (vi) inclusion in a thesis or dissertation; (vi) reuse of part of the article in another work (with citation); (vii) preparation of derivative works (with citation); (viii) voluntary posting on open websites operated by authors or author institutions for scientific purposes (follow the CC BY-SA License).
Authors and readers can copy and redistribute material in any media or format, and mix, modify, and build material for any purpose but they must provide appropriate credit (provide article citation or content), providing links to the license, and indicate if there are changes.
The authors submitting a manuscript do so on the understanding that if accepted for publication, copyright of the article shall be assigned to Jurnal Kimia Sains dan Aplikasi (JKSA). Copyright encompasses rights to reproduce and deliver the article in all form and media, including reprints, photographs, microfilms and any other similar reproductions, as well as translations.
Reproduce any part of this journal, its storage in the database or its transmission by all forms or media is permitted does not need for written permission from JKSA. However, it should be cited as an honor in academic manners
JKSA and the Chemistry Department of Diponegoro University and the Editor make every effort to ensure that there are no data, opinions, or false or misleading statements published in JKSA. However, the content of the article is the sole and exclusive responsibility of each author.
The Copyright Transfer Form can be downloaded here: [Copyright Transfer Form - Indonesian] [Copyright Transfer Form - English]. The copyright form should be signed originally and send to the Editor in the form of printed letters, scanned documents sent via email or fax.
Adi Darmawan, Ph.D (Editor in Chief)
Editor in chief of Jurnal Kimia Sains dan Aplikasi (JKSA)
Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University
Visitor: View My Stats
Jurnal Kimia Sains dan Aplikasi is indexed in:
This work is licensed under a Creative Commons Attribution-ShareAlike 4.0 International License.
