DOI: https://doi.org/10.14710/jksa.21.1.19-23

Blue Methylene Retrieval using Silica-Salicylic Acid Modified Filtering

Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University, Indonesia

Published: 31 Jan 2018.
Open Access Copyright 2018 Jurnal Kimia Sains dan Aplikasi under http://creativecommons.org/licenses/by-sa/4.0/.

Citation Format:
Abstract

The retrieval of methylene blue using a silica-modified sulfide-salicylic acid has been carried out. Salicylate-silica-acid alloys have been prepared by comparing the four media ie filter paper, silica-filter paper, salicylic acid-filter paper and salicylic acid-silica-filter paper. This study aims to study the recovery of methylene blue using salicylic acid-modified silica filtering with various parameters on the adsorption and desorption process. The results showed that the salicylic acid-silica alloy could improve the capability of methylene blue removal. The result of pH variation on the adsorption process showed that at pH 7 methylene blue can be taken 92.89%. Whereas at concentration variation, salicylic acid at 5 mM can take methylene blue equal to 92.86%. The desorption results showed that pH 1 methylene blue could be desorbed at 308.89 mg/g, while the variation of contact time of desorption ie at 110 minutes could an saturate the blue methylene by 589,61 mg/g. The UV-Vis analysis showed a decrease in absorbance in salicylic acid after contact with silica. The FTIR analysis also shows that in salicylate-silica-acid alloys there are Si-O groups derived from silica and C = O derived from salicylic acid.

Fulltext View|Download
Keywords: methylene blue; silica; salicylic acid

Article Metrics:

Article Info
Section: Research Articles
Language : EN
Recent articles
Synthesis of Zeolite from Sugar Cane as Detergent Builder: Variation of Si/Al Ratio and Hydrothermal TimeSynthesis of Zeolite from Sugar Cane as Detergent Builder: Variation of Si/Al Ratio and Hydrothermal Time Antibacterial Activity of Cinnamic Acid - Chitosan Encapsulation Synthesis and Antibacterial Testing of Imina Derivative Compounds from Piperonal and Anilin More recent articles
Most cited articles
Sintesis Asam Eugenoksi Asetat (EOA) dari Eugenol untuk Ekstraktan Logam Berat dan Recovery Krom dari Limbah Elektroplating Pengaruh Keasaman Medium dan Imobilisasi Gugus Organik pada Karakter Silika Gel dari Abu Sekam Padi Removal of natural organic matter for wetland saline water desalination by coagulation-pervaporation Sintesis Porous Carbon dari Sukrosa Menggunakan Silica Template pada Temperatur Kamar Pemanfaatan Montmorillonit Terpilar Al-Cr pada Adsorpsi Zat Warna Rhodamin B dengan Variasi Massa Adsorben dan Waktu Adsorpsi More cited articles
  1. Sulistias Mustika, Abdul Haris, Nor Basid Adiwibawa Prasetya, Kajian Metode Elektrofotokatalisis, Elektrolisis dan Fotokatalisis pada Dekolorisasi Larutan Zat Warna Remazol Black B yang Mengandung Ion Logam Cu2+, Jurnal Kimia Sains dan Aplikasi, 16, 1, (2013) 17-22
  2. Arthias Cita Febriyani, Rum Hastuti, Abdul Haris, Kajian Metode Elektrofotokatalisis, Elektrolisis dan Fotokatalisis pada Dekolorisasi Larutan Zat Warna Remazol Brilliant Orange 3R yang Mengandung Ion Logam Cu2+, Jurnal Kimia Sains dan Aplikasi, 15, 1, (2012) 7-12
  3. E.-S.Z. El-Ashtoukhy, Y.O Fouad, Liquid–liquid extraction of methylene blue dye from aqueous solutions using sodium dodecylbenzenesulfonate as an extractant, Alexandria Engineering Journal, 54, (2015) 77-81 10.1016/j.aej.2014.11.007
  4. Reza S. Razmara, Ali Daneshfar, Reza Sahrai, Determination of methylene blue and sunset yellow in wastewater and food samples using salting-out assisted liquid–liquid extraction, Journal of Industrial and Engineering Chemistry, 17, 3, (2011) 533-536 http://dx.doi.org/10.1016/j.jiec.2010.10.028
  5. Hekun Han, Wei Wei, Zhifeng Jiang, Junwei Lu, Jianjun Zhu, Jimin Xie, Removal of cationic dyes from aqueous solution by adsorption onto hydrophobic/hydrophilic silica aerogel, Colloids and Surfaces A: Physicochemical and Engineering Aspects, 509, Supplement C, (2016) 539-549 http://dx.doi.org/10.1016/j.colsurfa.2016.09.056
  6. W. H. Rahmanto, Muhammad Asy'ari, Sel Elektrolisis 3–Kompartemen untuk Ekstraksi Magnesium dan Sulfat dari Sistem Larutan MgSO4–KCl–H2O, Jurnal Kimia Sains dan Aplikasi, 9, 1, (2006)
  7. M. Soniya, G. Muthuraman, Comparative study between liquid–liquid extraction and bulk liquid membrane for the removal and recovery of methylene blue from wastewater, Journal of Industrial and Engineering Chemistry, 30, (2015) 266-273 http://dx.doi.org/10.1016/j.jiec.2015.05.032
  8. Reza Hosseinzadeh, Khatereh Khorsandi, Maryam Jahanshiri, Combination photodynamic therapy of human breast cancer using salicylic acid and methylene blue, Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy, 184, Supplement C, (2017) 198-203 http://dx.doi.org/10.1016/j.saa.2017.05.008
  9. Yasemin Bulut, Haluk Aydın, A kinetics and thermodynamics study of methylene blue adsorption on wheat shells, Desalination, 194, 1, (2006) 259-267 http://dx.doi.org/10.1016/j.desal.2005.10.032
  10. Robert M. Silverstein, Francis X. Webster, David J. Kiemle, David L. Bryce, Spectrometric Identification of Organic Compounds, 5 ed., John Wiley and Sons Inc., New York, 1991
  11. Shofi Dwika Adha, Danar Purwonugroho, Rachmat Triandi Tjahjanto, Pengaruh Konsentrasi Larutan HNO3 dan Waktu Kontak Terhadap Desorpsi Kadmium(II) yang Terikat Pada Biomassa Azolla Microphylla-Sitrat, Jurnal Ilmu Kimia Universitas Brawijaya, 1, 1, (2015) 636-642

Last update:

  1. Isotherm and kinetic modeling of Cr(VI) removal with quaternary ammonium functionalized silica

    Fatma Fakhfakh, Sahar Raissi, Fatma Ben Jeddou, Raida Zribi Zghal, Abdelhamid Ghorbel. Journal of Sol-Gel Science and Technology, 111 (3), 2024. doi: 10.1007/s10971-024-06492-9

  2. Removal of Methylene Blue Using Used Paper Powder

    Ghina Labiebah, Gunawan Gunawan, Muhammad Cholid Djunaidi, Abdul Haris, Didik Setiyo Widodo. Jurnal Kimia Sains dan Aplikasi, 22 (1), 2019. doi: 10.14710/jksa.22.1.23-28

Last update: 2024-11-13 15:49:10

No citation recorded.